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Pure Appl. Chem., 2011, Vol. 83, No. 3, pp. 479-487

http://dx.doi.org/10.1351/PAC-CON-10-09-05

Published online 2010-12-15

Improved synthesis of Bn5CpRu(CO)2Cl and its application as racemization catalyst in preparative-scale metalloenzymatic dynamic kinetic resolution of 1-phenylethanol

Denys Mavrynsky1, Liisa T. Kanerva2*, Reijo Sillanpää3 and Reko Leino1*

1 Laboratory of Organic Chemistry, Åbo Akademi University, 20500 Åbo, Finland
2 Laboratory of Synthetic Drug Chemistry and Department of Chemistry, University of Turku, 20014 Turku, Finland
3 Department of Chemistry, University of Jyväskylä, 40351 Jyväskylä, Finland

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  • Mavrynsky Denys, Murzin Dmitry Yu., Leino Reko: Kinetic Studies on sec -Alcohol Racemization with Dicarbonylchloro(pentabenzylcyclopentadienyl)- and Dicarbonylchloro(pentaphenylcyclopentadienyl)ruthenium Catalysts. ChemCatChem 2013, 5, 2436. <http://dx.doi.org/10.1002/cctc.201300163>
  • Mavrynsky Denys, Rahkila Jani, Bandarra Daniel, Martins Soraia, Meireles Margarida, Calhorda Maria José, Kovács Ida J., Zupkó István, Hänninen Mikko M., Leino Reko: Cytotoxicities of Polysubstituted Chlorodicarbonyl(cyclopentadienyl) and (Indenyl)ruthenium Complexes. Organometallics 2013, 32, 3012. <http://dx.doi.org/10.1021/om400234p>
  • Musa Musa M., Phillips Robert S., Laivenieks Maris, Vieille Claire, Takahashi Masateru, Hamdan Samir M.: Racemization of enantiopure secondary alcohols by Thermoanaerobacter ethanolicus secondary alcohol dehydrogenase. Org. Biomol. Chem. 2013, 11, 2911. <http://dx.doi.org/10.1039/c3ob27415b>
  • Marcos Rocío, Martín-Matute Belén: Combined Enzyme and Transition-Metal Catalysis for Dynamic Kinetic Resolutions. Isr. J. Chem. 2012, 52, 639. <http://dx.doi.org/10.1002/ijch.201200012>