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Pure Appl. Chem., 2008, Vol. 80, No. 8, pp. 1747-1762

http://dx.doi.org/10.1351/pac200880081747

High-temperature gradient HPLC and LC-NMR for the analysis of complex polyolefins

Harald Pasch, Lars-Christian Heinz, Tibor Macko and Wolf Hiller

German Institute for Polymers (Deutsches Kunststoff-Institut), Schlossgartenstr. 6, 64289 Darmstadt, Germany

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  • Mekap Dibyaranjan, Macko Tibor, Brüll Robert, Cong Rongjuan, deGroot Willem, Parrott Albert, Yau Wallace: Multiple-Injection Method in High-Temperature Two-Dimensional Liquid Chromatography (2D HT-LC). Macromol. Chem. Phys. 2014, 215, 314. <http://dx.doi.org/10.1002/macp.201300649>
  • Hiller Wolf, Sinha Pritish, Hehn Mathias, Pasch Harald: Online LC-NMR – From an expensive toy to a powerful tool in polymer analysis. Progress in Polymer Science 2013. <http://dx.doi.org/10.1016/j.progpolymsci.2013.10.001>
  • Weidner Steffen M., Falkenhagen Jana, Bressler Ingo: Copolymer Composition Determined by LC-MALDI-TOF MS Coupling and “MassChrom2D” Data Analysis. Macromol. Chem. Phys. 2012, 213, 2404. <http://dx.doi.org/10.1002/macp.201200169>
  • Macko Tibor, Brüll Robert, Wang Yongmei, Coto Baudilio, Suarez Inmaculada: Characterization of ethylene-propylene copolymers with high-temperature gradient adsorption liquid chromatography and CRYSTAF. J App Pol Sci 2011, 122, 3211. <http://dx.doi.org/10.1002/app.34432>
  • Macko Tibor, Brüll Robert, Alamo Rufina G., Stadler Florian J., Losio Simone: Separation of short-chain branched polyolefins by high-temperature gradient adsorption liquid chromatography. Anal Bioanal Chem 2011, 399, 1547. <http://dx.doi.org/10.1007/s00216-010-4335-y>
  • Macko Tibor, Brüll Robert, Zhu Yutian, Wang Yongmei: A review on the development of liquid chromatography systems for polyolefins. J Sep Science 2010, 33, 3446. <http://dx.doi.org/10.1002/jssc.201000516>
  • Macko Tibor, Pasch Harald, Wang Yongmei: Liquid Chromatographic Separation of Olefin Oligomers and its Relation to Separation of Polyolefins - an Overview. Macromol Symp 2009, 282, 93. <http://dx.doi.org/10.1002/masy.200950810>
  • Macko T., Brüll R., Alamo R.G., Thomann Y., Grumel V.: Separation of propene/1-alkene and ethylene/1-alkene copolymers by high-temperature adsorption liquid chromatography. Polymer 2009, 50, 5443. <http://dx.doi.org/10.1016/j.polymer.2009.09.057>