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Pure Appl. Chem., 2003, Vol. 75, No. 9, pp. 1239-1248

http://dx.doi.org/10.1351/pac200375091239

Polyhedral boron-containing cluster chemistry: Aspects of architecture beyond the icosahedron

Suzanne L. Shea1, Jonathan Bould1, Michael G. S. Londesborough1, Sarath D. Perera1,2, Andreas Franken1, Daniel L. Ormsby1, Tomás Jelínek1,3, Bohumil Stíbr3, Josef Holub1,3, Colin A. Kilner1, Mark Thornton-Pett1 and John D. Kennedy1

1 Department of Chemistry, University of Leeds, Leeds LS2 9JT, UK
2 Department of Chemistry, Open University, Nawala, Nugegoda, Sri Lanka
3 Institute of Inorganic Chemistry, Academy of Sciences of the Czech Republic, 25068 Rez-by-Prague, Czech Republic

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  • Chakrahari Kiran Kumarvarma, Sharmila Dudekula, Barik Subrat Kumar, Mondal Bijan, Varghese Babu, Ghosh Sundargopal: Hypoelectronic metallaboranes: Synthesis, structural characterization and electronic structures of metal-rich cobaltaboranes. Journal of Organometallic Chemistry 2014, 749, 188. <http://dx.doi.org/10.1016/j.jorganchem.2013.09.032>
  • Douvris Christos, Michl Josef: Update 1 of: Chemistry of the Carba-closo-dodecaborate(−) Anion, CB11H12–. Chem. Rev. 2013, 113, PR179. <http://dx.doi.org/10.1021/cr400059k>
  • Bould Jonathan, Macháček Jan, Londesborough Michael G. S., Macías Ramón, Kennedy John D., Bastl Zdeněk, Rupper Patrick, Baše Tomáš: Decaborane Thiols as Building Blocks for Self-Assembled Monolayers on Metal Surfaces. Inrog Chem 2012, 51, 1685. <http://dx.doi.org/10.1021/ic202000b>
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  • Carr Michael J., Clegg William, Kennedy John D., Londesborough Michael G. S., Kilner Colin A.: Macropolyhedral boron-containing cluster chemistry [S2B16H17]–. A new eighteen-vertex thiaborane anion. Collect Czech Chem Commun 2010, 75, 807. <http://dx.doi.org/10.1135/cccc2010053>
  • Scheschkewitz David: Eine neutrale, basenstabilisierte BB-Bindung: ein Lückenschluss. Angew Chem 2008, 120, 2021. <http://dx.doi.org/10.1002/ange.200705459>
  • Scheschkewitz David: A Base-Stabilized Neutral BB Bond: Closing a Gap by Filling the Void. Angew Chem Int Ed 2008, 47, 1995. <http://dx.doi.org/10.1002/anie.200705459>
  • Ormsby Daniel L., Greatrex Robert, Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. The reversible disassembly and reassembly of the hexagonal pyramidal {B7} feature in the [S2B18H19]− anion. Dalton Trans 2008, 1625. <http://dx.doi.org/10.1039/b715915c>
  • Jelínek Tomáš, Grüner Bohumir, Císařová Ivana, Štíbr Bohumil, Kennedy John D.: Macropolyhedral boron-containing cluster chemistry: The reaction of syn-B18H22 with SMe2 and I2 in monoglyme: Structure of [7-(SMe2)-syn-B18H20]. J Inorg Chem Commun 2007, 10, 125. <http://dx.doi.org/10.1016/j.inoche.2006.09.020>
  • Londesborough Michael G. S., Janou?ek Zbyn?k, ?t?br Bohumil, Hnyk Drahom?r, Ple?ek Jarom?r, C?sa?ov? Ivana: The [2,5,12-C3B8H15]? anion, the first representative of the eleven-vertex hypho family of tricarbaboranes. Dalton Trans 2007, 1221. <http://dx.doi.org/10.1039/b618082e>
  • Carr Michael J., Perera Sarath D., Jelínek Tomáš, Štíbr Bohumil, Clegg William, Kilner Colin A., Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. The unique nido-five-vertex-〈B2〉-nido-ten-vertex conjuncto structure of [(η5-C5Me5)2Rh2B11H15] via an unexpected cluster-dismantling. Chem Commun 2007, 3559. <http://dx.doi.org/10.1039/b709470a>
  • Bould Jonathan, Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. Novel intercluster linkages from the reaction of [Pt(cod)Cl2] and [PtMe2(PMe2Ph)2] with 6,6′-(B10H13)2O. Chem Commun 2007, 5084. <http://dx.doi.org/10.1039/b712084b>
  • Jelínek Tomáš, Císařová Ivana, Štíbr Bohumil, Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. Synthesis of the nineteen vertex monocarbaborane [9-(terBuNH2)-(anti)-9-CB18H20] by direct carbon-atom Aufbau. Dalton Trans 2007. <http://dx.doi.org/10.1039/b714631k>
  • Guo Qingliang, Dou Jianmin, Wu Libin, Li Dacheng, Daqiwang: Two iso-closo 11-vertex ruthenaborane clusters with exo-polyhedral cyclization of para-iodobenzoate. J Coord Chem 2007, 60, 785. <http://dx.doi.org/10.1080/00958970600918052>
  • Londesborough Michael G. S., Kilner Colin A., Kennedy John D.: Macropolyhedral Boron-Containing Cluster Chemistry. Intermolecular Coordination via Hydrogen-Metal Interaction. The Solvent-Free Synthesis and Dimeric Constitution of [Pd2B36H40(PMe2Ph)4]. Collect Czech Chem Commun 2007, 72, 1639. <http://dx.doi.org/10.1135/cccc20071639>
  • Dou Jianmin, Guo Qingliang, Wu Libin, Li Dacheng, Wang Daqi, Wang Huaisheng, Li Yantuan: Synthesis, crystal structure and electrochemical properties of threeisocloso eleven-vertex ferrocenecarboxylate ruthenaborane clusters. Appl Organometal Chem 2006, 20, 193. <http://dx.doi.org/10.1002/aoc.1031>
  • Guo Qing-Liang, Dou Jian-Min, Wu Li-Bin, Li Da-Cheng, Wang Da-Qi: Synthesis and Crystal Structure of Twoiso-closo 11-Vertexp-Bromobenzoate Ruthenoborane Clusters: [(PPh3)(p-BrC6H4CO2)2RuB10H8] and [(PPh3)2Ru(p-BrC6H4CO2)-(PPh3)RuB10H9]. Chin J Chem 2006, 24, 1741. <http://dx.doi.org/10.1002/cjoc.200690326>
  • Guo Qingliang, Dou Jianmin, Wu Libin, Li Dacheng, Wang Daqi, Wang Huaisheng: Synthesis and Crystal Structures of Twoexo-Cyclic 11-Vertexisocloso Ruthenaborane Clusters [(PPh3)(p-ClPhCO2)2RuB10H8] and [(PPh3)2Ru(PPh3)(p-ClPhCO2)RuB10H9]·0.5C5H12·H2O. Z anorg allg Chem 2006, 632, 1591. <http://dx.doi.org/10.1002/zaac.200600085>
  • Carr Michael J., Franken Andreas, Macías Ramón, Kennedy John D.: Twelve-vertex polyhedral carbaborane chemistry. Isostructural cations and anions: The ‘globule–globule’ salt [H3NCH2C2B10H11][H3CCH2CB11H11]. J Polyhedron 2006, 25, 1069. <http://dx.doi.org/10.1016/j.poly.2005.12.005>
  • Bould Jonathan, D?rfler Udo, Rath Nigam P., Barton Lawrence, Kilner Colin A., Londesborough Michael G. S., Ormsby Daniel L., Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. A synthetic approach via the auto-fusion of [6,9-(SMe2)2-arachno-B10H12]. Dalton Trans 2006, 3752. <http://dx.doi.org/10.1039/b604295c>
  • Carr Michael J., Londesborough Michael G. S., Hamilton Mcleod Alexander R., Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. Metallathiaboranes from S2B17H17: isolation and characterisation of [(?6-MeC6H4isoPr)RuS2B16H16] and [(?6-MeC6H4isoPr)RuS2B15H15]. Dalton Trans 2006, 3624. <http://dx.doi.org/10.1039/b607084c>
  • Franken Andreas, Jel?nek Tom??, Taylor Richard G., Ormsby Daniel L., Kilner Colin A., Clegg William, Kennedy John D.: Polyhedral monocarbaborane chemistry. Some C-phenylated seven, eight, nine, ten, eleven and twelve-vertex species. Dalton Trans 2006, 5753. <http://dx.doi.org/10.1039/b609908d>
  • Carr Michael J., Perera Sarath D., Jel?nek Tom??, Kilner Colin A., Clegg William, ?t?br Bohumil, Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. Cluster opening and B-frame rearrangement in the reaction of B16H20 with [{(IrCl2(?5-C5Me5)}2]. Synchrotron X-ray structures of [(?5-C5Me5)2Ir2B16H17Cl] and [(?5-C5Me5)2Ir2B16H15Cl]. Dalton Trans 2006, 5221. <http://dx.doi.org/10.1039/b611734a>
  • Dou Jianmin, Wu Libin, Guo Qingliang, Li Dacheng, Wang Daqi: A New Strategy for the Preparation of Metallaboranes − Solvothermal Synthesis and Structural Characterisation of Two Nido 11-vertex Diplatinaundecaborane Clusters. Eur J Inorg Chem 2005, 2005, 63. <http://dx.doi.org/10.1002/ejic.200400731>
  • Shea Suzanne L., MacKinnon Peter, Thornton-Pett Mark, Kennedy John D.: Macropolyhedral boron-containing cluster chemistry. Inorg Chim Ada 2005, 358, 1709. <http://dx.doi.org/10.1016/j.ica.2004.07.063>
  • Bould Jonathan, Bown Mark, Coldicott Richard J., Ditzel Evert J., Greenwood Norman N., Macpherson Ian, MacKinnon Peter, Thornton-Pett Mark, Kennedy John D.: Metallaborane reaction chemistry. Part 12. Some interactions of acetylenes and isocyanides with selected metallaboranes. J Organomet Chem 2005, 690, 2701. <http://dx.doi.org/10.1016/j.jorganchem.2005.02.028>
  • Bullen Neil J., Kennedy John D.: Polyhedral Monocarbaborane Chemistry. Functionality and Isomerism: Reactions of the [6-Ph-nido-6-CB9H11]- Anion with Aminopyridines NC5H4NH2 to Yield Neutral arachno and closo Ten-Vertex Monocarbaborane Derivatives. Collect Czech Chem Commun 2005, 70, 1873. <http://dx.doi.org/10.1135/cccc20051873>
  • Shea Suzanne L., Bould Jonathan, Londesborough Michael G. S., Perera Sarath D., Franken Andreas, Ormsby Daniel L., Jelinek Tomas, Stibr Bohumil, Holub Josef, Kilner Colin A.: Polyhedral Boron-Containing Cluster Chemistry: Aspects of Architecture Beyond the Icosahedron. ChemInform 2004, 35. <http://dx.doi.org/10.1002/chin.200404279>
  • Shea Suzanne L, Jelı́nek Tomáš, Perera Sarath D, Štı́br Bohumil, Thornton-Pett Mark, Kennedy John D: Macropolyhedral boron-containing cluster chemistry: two-electron variations in intercluster bonding intimacy. Contrasting structures of 19-vertex [(η5-C5Me5)HIrB18H19(PHPh2)] and [(η5-C5Me5)IrB18H18(PH2Ph)]. Inorg Chim Ada 2004, 357, 3119. <http://dx.doi.org/10.1016/j.ica.2004.03.041>