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Pure Appl. Chem., 2000, Vol. 72, No. 9, pp. 1715-1719

http://dx.doi.org/10.1351/pac200072091715

Titanacyclopropanes as versatile intermediates for carbon-carbon bond formation in reactions with unsaturated compounds

O. G. Kulinkovich

Department of Chemistry, Belarussian State University, Fr. Skaryny av., 4, Minsk, 220080, Belarus

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  • Setzer Paul, Forcher Gwénaël, Boeda Fabien, Pearson-Long Morwenna S. M., Bertus Philippe: Titanium-Mediated Addition of Grignard Reagents to Acyl Cyanohydrins: Aminocyclopropane versus 1,4-Diketone Formation. Eur. J. Org. Chem. 2014, 2014, 171. <http://dx.doi.org/10.1002/ejoc.201301251>
  • Li Wenjie, Gao Joe J., Lorenz Jon C., Xu Jinghua, Johnson Joe, Ma Shengli, Lee Heewon, Grinberg Nelu, Busacca Carl A., Lu Bruce: Process Development and Pilot-Plant Synthesis of (S)-tert-Butyl 1-Oxo-1-(1-(pyridin-2-yl)cyclopropylamino)propan-2-ylcarbamate: Studies on the Scale-Up of Kulinkovich–Szymoniak Cyclopropanation. Org Process Res Devel 2012, 16, 836. <http://dx.doi.org/10.1021/op300059b>
  • Setzer Paul, Beauseigneur Alice, Pearson-Long Morwenna S. M., Bertus Philippe: Titanium-Mediated Synthesis of 1,4-Diketones from Grignard Reagents and Acyl Cyanohydrins. Angew Chem 2010, 122, 8873. <http://dx.doi.org/10.1002/ange.201003923>
  • Setzer Paul, Beauseigneur Alice, Pearson-Long Morwenna S. M., Bertus Philippe: Titanium-Mediated Synthesis of 1,4-Diketones from Grignard Reagents and Acyl Cyanohydrins. Angew Chem Int Ed 2010, 49, 8691. <http://dx.doi.org/10.1002/anie.201003923>
  • Kulinkovich O. G.: ChemInform Abstract: Titanacyclopropanes as Versatile Intermediates for Carbon-Carbon Bond Formation in Reactions with Unsaturated Compounds. ChemInform 2010, 32, no. <http://dx.doi.org/10.1002/chin.200123276>
  • Wolan Andrzej, Six Yvan: Synthetic transformations mediated by the combination of titanium(IV) alkoxides and grignard reagents: selectivity issues and recent applications. Part 1: reactions of carbonyl derivatives and nitriles. Tetrahedron 2010, 66, 15. <http://dx.doi.org/10.1016/j.tet.2009.10.050>
  • Wolan Andrzej, Six Yvan: Synthetic transformations mediated by the combination of titanium(IV) alkoxides and Grignard reagents: selectivity issues and recent applications. Part 2: Reactions of alkenes, allenes and alkynes. Tetrahedron 2010, 66, 3097. <http://dx.doi.org/10.1016/j.tet.2010.01.079>
  • Concellón José M., Rodríguez-Solla Humberto, Blanco Elena G., Villa-García María A., Alvaredo Noemí, García-Granda Santiago, Díaz M. Rosario: Highly Stereoselective Halocyclopropanation of α,β-Unsaturated Amides. Adv Synth Catal 2009, 351, 2185. <http://dx.doi.org/10.1002/adsc.200900331>
  • Edson Joseph B., Keresztes Ivan, Lobkovsky Emil B., Coates Geoffrey W.: Alkene Polymerization Catalysts Bearing Tridentate Phenoxyamine Ligands with sp3 C Donors. ChemCatChem 2009, 1, 122. <http://dx.doi.org/10.1002/cctc.200900122>
  • Kulinkovich Oleg, Isakov Vladimir, Kananovich Dzmitry: Stereocontrolled alkylation of unsaturated compounds with alkoxytitanacyclopropane reagents. Chem Record 2008, 8, 269. <http://dx.doi.org/10.1002/tcr.20155>
  • Isakov Vladimir E., Kulinkovich Oleg G.: Highly stereoselective allylic ethylation with alkoxytitanacyclopropane reagents. Synthesis of (1R/S,7R)-1,7-dimethylnonyl propanoate, the Western corn rootworm sex attractant. Tetrahetron Lett 2008, 49, 6959. <http://dx.doi.org/10.1016/j.tetlet.2008.08.063>
  • Kulinkovich Oleg G., Kananovich Dzmitry G.: Advanced Procedure for the Preparation ofcis-1,2-Dialkylcyclopropanols – Modified Ate Complex Mechanism for Titanium-Mediated Cyclopropanation of Carboxylic Esters with Grignard Reagents. Eur J Org Chem 2007, 2007, 2121. <http://dx.doi.org/10.1002/ejoc.200601035>
  • Kulinkovich O. G., Shevchuk T. A., Isakov V. E., Prokhorevich K. N.: Reductive ethylation of homoallyl alcohols with a disubstituted double bond with ethylmagnesium bromide in the presence of titanium(IV) isopropoxide. Russ J Org Chem 2006, 42, 659. <http://dx.doi.org/10.1134/S1070428006050034>
  • Kulinkovich Oleg: Synthetic Applications of Intermolecular Cyclopropanation of Carboxylic Esters with Dialkoxytitanacyclopropane Reagents. Eur J Org Chem 2004, 2004, 4517. <http://dx.doi.org/10.1002/ejoc.200400234>