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Pure Appl. Chem., 1979, Vol. 51, No. 10, pp. 2005-2018

http://dx.doi.org/10.1351/pac197951102005

Direct electrochemical synthesis of inorganic and organometallic compounds

D. G. Tuck

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  • Casanova Isabel, Sousa-Pedrares Antonio, Viqueira Joaquin, Durán María L., Romero Jaime, Sousa Antonio, García-Vázquez José A.: Electrochemical synthesis and structural characterization of homoleptic and heteroleptic cobalt, nickel, copper, zinc and cadmium compounds with the 2-hydroxy-1,4-naphthoquinone ligand. New J. Chem. 2013, 37, 2303. <http://dx.doi.org/10.1039/c3nj00227f>
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  • Rodríguez Antonio, Sousa-Pedrares Antonio, García-Vázquez José A., Romero Jaime, Sousa Antonio: Electrochemical synthesis and characterization of zinc(II) complexes with pyrimidine-2-thionato ligands and their adducts with N,N donors. J Polyhedron 2009, 28, 2240. <http://dx.doi.org/10.1016/j.poly.2009.03.029>
  • Labisbal Elena, Rodríguez Laura, Souto Oscar, Sousa-Pedrares Antonio, García-Vázquez José Arturo, Romero Jaime, Sousa Antonio, Yáñez Matilde, Orallo Francisco, Real José A.: Electrochemical synthesis and structural characterization of Co(II), Ni(II) and Cu(II) complexes of N,N-bis(4,5-dimethyl-2-hydroxybenzyl)-N-(2-pyridylmethyl)amine. Dalton Trans 2009, 8644. <http://dx.doi.org/10.1039/b907539a>
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  • Cabaleiro Santiago, Calvo Rafael, Castro Jesús, García-Vázquez J. Arturo, Napolitano Lia M. B., Nascimento Otaciro R., Pérez-Lourido Paulo, Romero Jaime, Sousa Antonio: Synthesis and Structure of the Dimeric Copper(II) Complex Tetrakis[N-thiazol-2-yl-(4-methylphenyl)sulfonamidate]dicopper(II). J Chem Crystallogr 2008, 38, 71. <http://dx.doi.org/10.1007/s10870-007-9303-9>
  • Sousa-Pedrares Antonio, Camiña Nuria, Romero Jaime, Durán Maria L., García-Vázquez José A., Sousa Antonio: Electrochemical synthesis and crystal structure of cobalt(II), nickel(II), copper(II), zinc(II) and cadmium(II) complexes with 2-pyridinecarbaldehyde-(2′-aminosulfonylbenzoyl)hydrazone. J Polyhedron 2008, 27, 3391. <http://dx.doi.org/10.1016/j.poly.2008.08.011>
  • Rodríguez A., García-Vázquez José Arturo, Romero J., Sousa-Pedrares A., Sousa A., Castro J.: Electrochemical Synthesis and Characterization of Cobalt(II), Cobalt(III), and Nickel(II) Complexes with Pyrimidine-2-thionato Ligands. Z anorg allg Chem 2007, 633, 763. <http://dx.doi.org/10.1002/zaac.200600387>
  • Ren Zhi-Gang, Tang Xiao-Yan, Li Li, Liu Guang-Fei, Li Hong-Xi, Chen Yang, Zhang Yong, Lang Jian-Ping: Electrochemical syntheses and structures of lead(II) and bismuth(III) complexes of 4-(trimethylammonio)benzenethiolate. J Inorg Chem Commun 2007, 10, 1253. <http://dx.doi.org/10.1016/j.inoche.2007.08.004>
  • Kharisov Boris I., Garnovskii Alexander D., Kharissova Oxana V., Méndez Ubaldo Ortiz, Tsivadze Aslan Yu.: Direct electrochemical synthesis of metal complexes of phthalocyanines and azomethines as model compounds: advantages and problems of this method versus traditional synthetic techniques. J Coord Chem 2007, 60, 1435. <http://dx.doi.org/10.1080/00958970601040658>
  • Beloso Inmaculada, Castro Jesús, García-Vázquez José A., Pérez-Lourido Paulo, Romero Jaime, Sousa Antonio: Electrochemical synthesis and structural characterization of heteroleptic cobalt(II) complexes of N-2-pyridyl sulfonamide ligands. J Polyhedron 2006, 25, 2673. <http://dx.doi.org/10.1016/j.poly.2006.03.004>
  • Frolov V. Yu., Bolotin S. N., Panyshkin V. T.: Electrochemical Synthesis of Complex Compounds of Transition Elements with Carboxyl- and Carbonyl-containing Ligands. Russ J Appl Chem 2005, 78, 897. <http://dx.doi.org/10.1007/s11167-005-0416-7>
  • Yuan Yaxian, Yao Jianlin, Lu Jun, Zhang Yong, Gu Renao: Direct electrochemical synthesis and crystal structure of a copper(II) complex with a chiral (S)-2-(diphenylmethanol)-l-(2-pyridylmethyl)pyrrolidine. J Inorg Chem Commun 2005, 8, 1014. <http://dx.doi.org/10.1016/j.inoche.2005.08.006>
  • García-Vázquez José A., Sousa-Pedrares Antonio, Carabel Maximiliano, Romero Jaime, Sousa Antonio: Electrochemical synthesis and structural characterization of copper and silver complexes of imidazolidine-2-thione ligands. J Polyhedron 2005, 24, 2043. <http://dx.doi.org/10.1016/j.poly.2005.06.016>
  • Yuan Yaxian, Yao Jianlin, Lin Cheng, Zhang Yong, Gu Renao: Direct Electrochemical Synthesis and Crystal Structure of Copper(I) Complex with 2′‐hydroxy‐5′‐methyl‐acetophenone and Triphenylphosphine Ligands. Synthesis & Reactivity in Inorg Metal-Org & Nano-Metal Chem 2005, 35, 385. <http://dx.doi.org/10.1081/SIM-200059211>
  • Beloso Inmaculada, Castro Jesús, García—Vázquez José A., Pérez—Lourido Paulo, Romero Jaime, Sousa Antonio: Different Coordinative (N, N) and (N, O) Bidentate Behaviour of N-2-Pyridyl-Sulfonamides. Electrochemical Synthesis and Characterization of Cadmium(II) Complexes. Z anorg allg Chem 2003, 629, 275. <http://dx.doi.org/10.1002/zaac.200390044>
  • Favier Isabelle, Duñach Elisabet: Novel electrosynthesis of metallic bis(trifluoromethanesulfonyl) imides. Tetrahetron Lett 2003, 44, 2031. <http://dx.doi.org/10.1016/S0040-4039(03)00214-4>
  • Garnovskii D.A., Guedes da Silva M.F.C., Kopylovich M.N., Garnovskii A.D., Fraústo da Silva J.J.R., Pombeiro A.J.L.: Electrochemical synthesis of adducts of 2-aminopyridine or methanol in metal chelates of a N,N,N-tridentate Schiff base ligand. X-ray crystal structures of the Ni(II) and Zn(II) derivatives. J Polyhedron 2003, 22, 1335. <http://dx.doi.org/10.1016/S0277-5387(03)00104-9>
  • Garnovskii D. A., Sadikov G. G., Antsyshkina A. S., Burlov A. S., Vasil’chenko I. S., Garnovskaya E. D., Sergienko V. S., Garnovskii A. D.: Adducts of metallochelate complexes of tridentate N,N,N-donating azomethine ligands: Crystal structures of (2-aminopyridine)[2-N-tosylamino(2′-tosylaminobenzal)anilinato]nickel(II) and (methanol)[2-N-tosylamino(2′-tosylaminobenzal)anilinato]copper(II). Crystallogr Rep 2003, 48, 426. <http://dx.doi.org/10.1134/1.1578127>
  • Boyle Philip D., Godfrey Stephen M.: The reactions of sulfur and selenium donor molecules with dihalogens and interhalogens. Coord Chem Rev - 2001, 223, 265. <http://dx.doi.org/10.1016/S0010-8545(01)00386-1>
  • Cabaleiro Santiago, Castro* Jesús, Garcı́a-Vázquez José A, Romero Jaime, Sousa* A: Direct electrochemical synthesis of cobalt(II) complexes of tosylamides: crystal structures of [CoL2py2], [CoL2DMF2], [CoL2bipy] and [CoL2phen], L=[(4-methylphenyl)sulfonyl]-2-pyridylamide. J Polyhedron 2000, 19, 1607. <http://dx.doi.org/10.1016/S0277-5387(00)00437-X>
  • Garcı́a-Vázquez José A., Romero Jaime, Sousa Antonio: Electrochemical synthesis of metallic complexes of bidentate thiolates containing nitrogen as an additional donor atom. Coord Chem Rev - 1999, 193-195, 691. <http://dx.doi.org/10.1016/S0010-8545(99)00046-6>
  • Cabaleiro Santiago, Vázquez-López Ezequiel, Castro Jesús, Garcı́a-Vázquez José A, Romero Jaime, Sousa Antonio: Cadmium(II) complexes with [(4-methylphenyl)sulfonyl]-2-pyridyl-amine: crystal structures of bis{[(4-methylphenyl)sulfonyl]-2-pyridyl-amide}cadmium(II); aquo-bis(pyridine) bis{[(4-methylphenyl)sulfonyl]-2-pyridyl-amide}cadmium(II) and 1,10-phenanthroline bis{[(4-methylphenyl)sulfonyl]-2-pyridyl-amide}cadmium(II). Inorg Chim Ada 1999, 294, 87. <http://dx.doi.org/10.1016/S0020-1693(99)00265-0>
  • Méndez-Rojas Miguel A., Cordova-Lozano Felipe, Gojon-Zorrilla Gabriel, González-Vergara Enrique, Quiroz Marco A.: Direct electrosynthesis of Cu, Cd, Zn complexes of piroxicam (4-hydroxy-2-methyl-N-(2-pyridyl)-2H-1,2-benzothiazine-3-carboxamide-1,1,-dioxide) and isoxicam (4-hydroxy-2-methyl-N-(5-methyl-3-isoxazolyl)-2H-1,2-benzothiazine-3-carboxamide-1,1-dioxide) in nonaqueous media by in-situ generation of supporting electrolyte. J Polyhedron 1999, 18, 2651. <http://dx.doi.org/10.1016/S0277-5387(99)00172-2>
  • Kharisov B. I., Blanco L. M., Salinas M. V., Garnovskii A. D.: DIRECT SYNTHESIS OF COPPER DIMETHYLDITHIOCARBAMATE DERIVATIVES: AN OPTIMIZATION USING ULTRASONIC TREATMENT. J Coord Chem 1999, 47, 135. <http://dx.doi.org/10.1080/00958979908024548>
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  • Hayes Peter C., Osman Akhtar, Seudeal Narace, Tuck Dennis G.: The direct electrochemical synthesis of 2,2′-bipyridine adducts of organomagnesium halides, and of salts of organodihalogenomagnesium(II) anions. J Organomet Chem 1985, 291, 1. <http://dx.doi.org/10.1016/0022-328X(85)80197-2>
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  • Nishimura Edward K., Filgueiras Carlos A.L., Celso Celio, Coelho Geraldo H., Johnson Brian F.G., Hencher J.Lawrence, Khan Masood, Said Farouq F., Tuck Dennis G.: Skeletal electron counting in transition metal heteroboranes and related species. Inorganic and Nuclear Chemistry Letters 1981, 17, 269. <http://dx.doi.org/10.1016/0020-1650(81)80077-3>
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