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Pure Appl. Chem., 1988, Vol. 60, No. 8, pp. 1185-1192

Structure and reactivity of molybdenum clusters with loose coordination site, Mo3[S4P(OEt)2]4L

J. Q. Huang, J. L. Huang, M. Y. Shang, S. F. Lu, X. T. Lin, Y. H. Lin, M. D. Huang, H. H. Zhuang and J. X. Lu

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  • Gushchin A. L., Laricheva Yu. A., Piryazev D. A., Sokolov M. N.: Mixed-ligand cluster [Mo3S4(Dtp)2(μ-AcO)Cl(Me2Bipy)]: Synthesis and structure. Russ J Coord Chem 2014, 40, 5. <>
  • Hernandez-Molina Rita, Gushchin Artem, González-Platas Javier, Martínez Manuel, Rodríguez Carlos, Vicent Cristian: Tungsten and molybdenum incomplete cuboidal clusters; kinetico-mechanistic studies and association in dimers. Dalton Trans. 2013, 42, 15016. <>
  • Yoshida Ryouichi, Shibahara Takashi, Akashi Haruo: Synthesis and Characterization of Oxygen/Sulfur-Bridged Incomplete Cubane-Type Clusters, [M3S4(Tpe)3]+ and [M3OS3(Tpe)3]+ (M = Mo and W), and a Mixed-Metal Cubane-Type Cluster, [Mo3PdS4Cl(Tpe)3]. Bull. Chem. Soc. Jpn. 2013, 86, 839. <>
  • Hernandez-Molina Rita, Gonzalez-Platas Javier, Kovalenko Konstantin A., Sokolov Maxim N., Virovets Alexandre V., Llusar Rosa, Vicent Cristian: Cuboidal Mo3S4 and Mo3NiS4 Complexes Bearing Dithiophosphates and Chiral Carboxylate Ligands: Synthesis, Crystal Structure and Fluxionality. Eur J Inorg Chem 2011, 2011, 683. <>
  • Chen Zhi-Da, Lu Jia-Xi, Li Jun, Liu Chun-Wan, Zhang Qian-Er: A comparative study of the aromaticity in some typical conjugated six-membered rings by the method of localized molecular orbital. Chin J Chem 2010, 9, 385. <>
  • Lu Shao-Fang, Huang Zi-Xiang, Huang Jian-Quan, Zhang Bin, Huang Jin-Ling: Synthesis and structure of an open-type trinuclear molybdenum cluster compound [Mo3(μ3-S)(μ-S)2-(μ-OAc)(S2CNC4H8)3(O)2] · 0.5CH2Cl2 · 2H2O. Chin J Chem 2010, 10, 52. <>
  • Lu Shao-Fang, Huang Jian-Quan, Huang Zi-Xiang, Zhang Bin, Huang Jin-Ling: The synthesis and crystal structure of a trinuclear molybdenum cluster compound [Mo3(μ-O)(μ-S)3(μ(μ-OAc)2(dtp)2·(Py)]·0.5H2O. Chin J Chem 2010, 10, 500. <>
  • Li Jun, Liu Chun-Wan, Lu Jia-Xi: Localized molecular orbital studies of certain compounds with [A3X3] six-membered rings. Chin J Chem 2010, 11, 481. <>
  • Li Zhao-Ji, Qin Ye-Yan, Tang Yan-Hong, Kang Yao, Xia Ji, Chen Zhong, Wu Ling, Yao Yuan-Gen: P NMR studies on the ligand dissociation of trinuclear molybdenum cluster compounds. Chin J Chem 2010, 21, 1174. <>
  • Perera Eranda, Basu Partha: Synthesis, characterization and structure of a low coordinate desoxomolybdenum cluster stabilized by a dithione ligand. Dalton Trans 2009, 5023. <>
  • Tang Yan-Hong, Qin Ye-Yan, Li Zhao-Ji, Zhang Jian, Kang Yao, Hu Rui-Feng, Wen Yi-Hang, Cheng Jian-Kai, Yao Yuan-Gen: Syntheses, Crystal Structures of Mo–S Clusters [Mo3S4(dtp)3(L)]2[μ-OOC(CH2)nCOO-μ] (L = dmf, dmso; n = 3, 4) and Their Supramolecular Architectures. Bull Chem Soc Jpn 2005, 78, 626. <>
  • Chen Yu-Biao, Wen Yi-Hang, Qin Ye-Yan, Kang Yao, Li Zhao-Ji, Cheng Jian-Kai, Yao Yuan-Gen: Dimerization of trinuclear molybdenum (IV) clusters. J Inorg Chem Commun 2004, 7, 718. <>
  • Qin Ye-Yan, Yao Yuan-Gen, Kang Yao, Li Zhao-Ji, Chen Yu-Biao: A Neutral Trinuclear Molybdenum-Sulfur(Oxygen) Cluster Complex with [Mo3(μ3-S)(μ-O)3] Core. Chem Lett 2002, 1024. <>
  • Chen Huayang, Lin Xiang, Chi Lisheng, Lu Canzhong, Zhuang Honghui, Huang Jinshun: Synthesis and crystal structures of new triangle tungsten telluride compounds containing a [W3(μ3-Te)(μ2-Te2)3]4+ cluster core: {W3Te7[(RO)2PS2]3}I (R=Et, Pri). J Inorg Chem Commun 2000, 3, 331. <>
  • Haruo Akashi, Takashi Shibahara: Preparation and characterization of twin-cubane-type clusters with molybdenum-copper-sulfur cores: X-ray structure determination of [{(NH3)6(H2O)(OH)Mo3CuS4(O)}2]Cl4·8H2O. Inorg Chim Ada 1998, 282, 50. <>
  • Huang Jian-Quan, Lu Shao-Fang, Huang Xiao-Ying, Wu Qiang-Jin, Yu Rong-Min: The synthesis and crystal structure of novel Mo-Sn tetranuclear cubane-like cluster [Mo3(SnBr3)(μ3-O)(μ3-S)3(dtp)3(py)3]·(CH2Cl2). J Clust Sci 1997, 8, 47. <>
  • Zhuang Botao, Yu Peihua, Huang Liangren, He Lingjie, Pan Guohua: A novel pentanuclear CoS raft cluster compound consisting of fused Co3(μ3-S) units: X-ray crystal structure of Co5(CO)2S3(SC5H4N)7. J Polyhedron 1997, 16, 1425. <>
  • Saito Taro, Imoto Hideo: Chalcogenide Cluster Complexes of Chromium, Molybdenum, Tungsten, and Rhenium. Bull Chem Soc Jpn 1996, 69, 2403. <>
  • Chen Zhida: Multicentered bonding and quasi-aromaticity in metal-chalcogenide cluster chemistry. J Clust Sci 1995, 6, 357. <>
  • Saysell David M., Sykes A. Geoffrey: Heterometallic cuboidal complexes as derivatives of the [MO3S4(H2O)9]4+ cluster. J Clust Sci 1995, 6, 449. <>
  • Lu Shao-Fang, Chen Hong-Bing, Huang Jian-Quan, Wu Qiang-Jin, Sun Qiong-Li, Li Jun, Lu Jia-Xi: Ligand-cluster reactivity and structure relationship; the synthesis, structural characterization and properties of two new MoCuS cluster compounds. Inorg Chim Ada 1995, 232, 43. <>
  • Haiduc Ionel, Sowerby D.Bryan, Lu Shao-Fang: Stereochemical aspects of phosphor-1,1-dithiolato metal complexes (dithiophosphates, dithiophosphinates): Coordination patterns, molecular structures and supramolecular associations—I. J Polyhedron 1995, 14, 3389. <>
  • Shibahara Takashi, Sakane Genta, Naruse Yoshiyuki, Taya Kazuhisa, Akashi Haruo, Ichimura Akio, Adachi Hirohiko: Syntheses and Characterization of Cubane-Type Clusters with Molybdenum-Iron-Sulfur (Mo3FeS4) or Molybdenum-Nickel-Sulfur (Mo3NiS4) Cores. X-Ray Structures of (Mo3FeS4(H2O)10)(CH3C6H4SO3)47H2O and (Mo3FeS4(H2O)(NH3)9)Cl4, and Discrete Variational (DV)-X.ALPHA. Calculation of the Electronic Structures of (Mo3FeS4(H2O)10)4+, (Mo3FeS4(H2O)(NH3)9)4+, and (Mo3NiS4(H2O)10)4+. Bull Chem Soc Jpn 1995, 68, 2769. <>
  • Diller H., Keck H., Wunderlich H., Kuchen W.: Periphere Anbindung von Quecksilber(II)-iodid an dreikernige Molybdän-Schwefel-Dithiophosphinatocluster: [Mo3S4(R2PS2)4HgI2] (R = Et, Pr). Z anorg allg Chem 1994, 620, 1422. <>
  • Li Jun, Liu Chun-Wan, Lu Jia-Xi: Quantum chemical studies on the bonding characteristics of some M3X4 transition-metal halogenide clusters. J Clust Sci 1994, 5, 505. <>
  • Li Jun, Liu Chun-Wan, Lu Jia-Xi: Electronic structures and dpπ bonding of some M3X4+4 cluster compounds. J Polyhedron 1994, 13, 1841. <>
  • Lu Jia-Xi, Chen Zhi-Da: Novel quasi-aromatic transition metal cluster compounds. Int Rev Phys Chem 1994, 13, 85. <>
  • Cheng Wen-Dan, Huang Jin-Shun, Zhang Qian-Er: Electronic structure of the ground state and calculated spectrum of low-lying excited states of Mo3X4(aq)4+9 (X=O, S) cluster ions. chem phys letts 1993, 216, 353. <>
  • Shibahara Takashi: Syntheses of sulphur-bridged molybdenum and tungsten coordination compounds. Coord Chem Rev - 1993, 123, 73. <>
  • Cotton F.Albert, Maoyu Shang, Zhong Sheng Sun: Preparation of the new species [W3(μ3-O)(μ-Cl)2(μ-O2CMe)4Cl3]− and [Mo3(μ3-O)(μ-Cl)4(μO2CMe)2Cl2(PMe3)2]− that bracket, structurally, the very common M3(μ3-O)(μ-X)3(μ-O2CR3)3L3 type of cluster compound. Inorg Chim Ada 1993, 212, 95. <>
  • Zhi-da Chen, Jia-xi Lu, Chun-wan Liu, Qian-er Zhang: A localized molecular orbital study on the bonding of > Mo3S4]2Mo >8+ and > Mo3S4]CuI >4+ versus (C6H6)2Cr and C6H6Cr(CO)3. Journal of Molecular Structure: THEOCHEM 1991, 236, 343. <>
  • Fedin V.P., Sokolov M.N., Geras'ko O.A., Virovets A.V., Podberezskaya N.V., Fedorov V.Ye.: Triangular M3Se74+ and M3Se44+ complexes (M = Mo, W). An X-ray study of Mo3Se7(Et2NCS2)4 and W3Se7(Et2NCS2)4. Inorg Chim Ada 1991, 187, 81. <>
  • Chen Zhida, Lu Jiaxi, Liu Chunwan, Zhang Qianer: Localized molecular orbitals and the problem of quasi-aromaticity in trinuclear molybdenum cluster compounds with cores of the type [MO3(μ3-X)(μ-Y)3]n+ (X, Y = O, S, n = 4; X = O, Y = Cl, n = 5). J Polyhedron 1991, 10, 2799. <>
  • Shibahara Takashi, Akashi Haruo, Yamasaki Mikio, Hashimoto Kohichi: Reaction of (Mo3S4(H2O)9)4+ with cobalt and mercury. Syntheses and X-ray structures of double cubane-type cluster, ((H2O)9Mo3S4CoCoS4Mo3(H2O)9)(CH3C6H4SO3)818H2O and sandwich cubane-type cluster, ((H2O)9Mo3S4HgS4Mo3(H2O)9)(CH3C6H4SO3)820H2O. Chem Lett 1991, 689. <>
  • Keller Thomas, Zimmermann Heinrich, Schneider Walter, Schmalle Helmut, Dubler Erich, Hegetschweiler Kaspar: A new synthetic pathway for tris-μ-disulfido-μ3-thio-triangulo-trimolybdenum(IV) complexes: preparation, characterization and structure of [Mo3S(S2)3(OOCCHSCH2COOH)3]2−. Inorg Chim Ada 1990, 169, 235. <>