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Pure Appl. Chem., 1984, Vol. 56, No. 7, pp. 807-819

http://dx.doi.org/10.1351/pac198456070807

Structural analysis of blood-group ABH, I, i, Lewis and related glycosphingolipids. Application of FAB mass spectrometry and high resolution proton NMR

H. Egge, Janusz Dabrowski and Peter Hanfland

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  • Bergqvist Magnus, Holmbäck Jan: Nuclear magnetic resonance spectroscopy and reversed-phase high-performance liquid chromatography of peracetylated digalactosyldiacylglycerols. J Amer Oil Chem Soc 2000, 77, 757. <http://dx.doi.org/10.1007/s11746-000-0121-6>
  • Matsuzaki Yuji, Ito Yukishige, Nakahara Yoshiaki, Ogawa Tomoya: Synthesis of branched poly-N-acetyl-lactosamine type pentaantennary pentacosasaccharide: Glycan part of a glycosyl ceramide from rabbit erythrocyte membrane. Tetrahetron Lett 1993, 34, 1061. <http://dx.doi.org/10.1016/S0040-4039(00)77492-2>
  • Dell Anne, Morris Howard R., Greer Fiona, Redfern Joanne M., Rogers Mark E., Weisshaar Gerhard, Hiyama Jun, Renwick Alistair G.C.: Fast-atom-bombardment mass spectrometry of sulphated oligosaccharides from ovine lutropin. Carbohydrates Research 1991, 209, 33. <http://dx.doi.org/10.1016/0008-6215(91)80143-B>
  • Dell Anne, Azadi Parastoo, Tiller Philip, Thomas-Oates Jane, Jennings Harold J., Beurret Michel, Michon Francis: Analysis of oligosaccharide epitopes of meningococcal lipopolysaccharides by fast-atom-bombardment mass spectrometry. Carbohydrates Research 1990, 200, 59. <http://dx.doi.org/10.1016/0008-6215(90)84182-T>
  • Narasinga Rao B.N., Allen Bush C.: The determination of the structure of blood group oligosaccharides from fully assigned 1H-n.m.r. spectra for solutions in non-aqueous solvents. Carbohydrates Research 1988, 180, 111. <http://dx.doi.org/10.1016/0008-6215(88)80068-5>
  • Dabrowski Janusz, Hauck Michael, Romanowska Elzbieta, Gamian Andrzej: Structure elucidation of the core octasaccharide from Citrobacter PCM 1487 with the aid of 500-MHz, two-dimensional phase-sensitive correlated, relayed-coherence transfer, double-quantum, triple-quantum filtered, and N.O.E. 1H-n.m.r. spectra. Carbohydrates Research 1988, 180, 163. <http://dx.doi.org/10.1016/0008-6215(88)80074-0>
  • Hanfland Peter, Kordowicz Maria, Peter-Katalinić Jasna, Egge Heinz, Dabrowski Janusz, Dabrowski Ursula: Structure elucidation of blood group B-like and I-active ceramide eicosa- and pentacosa-saccharides from rabbit erythrocyte membranes by combined gas chromatography-mass spectrometry; electron-impact and fast-atom-bombardment mass spectrometry; and two-dimensional correlated, relayed-coherence transfer, and nuclear overhauser effect 500-MHz 1H-N.m.r. spectroscopy. Carbohydrates Research 1988, 178, 1. <http://dx.doi.org/10.1016/0008-6215(88)80098-3>
  • Egge Heinz, Peter-Katalinić Jasna: Fast atom bombardment mass spectrometry for structural elucidation of glycoconjugates. Mass Spectrom Rev 1987, 6, 331. <http://dx.doi.org/10.1002/mas.1280060302>
  • Dabrowski Janusz, Dabrowski Ursula, Hanfland Peter, Kordowicz Maria, Hull William E.: Structure determination of peracetylated glycosphingolipids by one- and two-dimensional1H NMR at 360 and 500 MHz. Magn Reson Chem 1986, 24, 59. <http://dx.doi.org/10.1002/mrc.1260240113>
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  • Bélanger Jacqueline, Paré J.R.Jocelyn: Fast atom bombardment mass spectrometry in the pharmaceutical analysis of drugs. J  Pharm Biomed Anal 1986, 4, 415. <http://dx.doi.org/10.1016/0731-7085(86)80064-4>
  • ROMANOWSKA Elzbieta, GAMIAN Andrzej, DABROWSKI Janusz: Core region of Citrobacter lipopolysaccharide from strain PCM 1487. Structure elucidation by two-dimensional 1H-NMR spectroscopy at 500 MHz and methylation analysis/mass spectrometry. Eur J Biochem 1986, 161, 557. <http://dx.doi.org/10.1111/j.1432-1033.1986.tb10478.x>
  • Peter-Katalinić J., Reuter G., Schauer R., Ghidoni R., Sonnino S., Tettamanti G., Egge H.: Analysis of gangliosides using fast atom bombardment mass spectrometry. J Chem Phys Lipids 1985, 37, 127. <http://dx.doi.org/10.1016/0009-3084(85)90080-5>